Detail mata kuliah Karakterisasi Material + Lab, program studi S2 - Teknik Metalurgi dan Material

Detail SAP: Karakterisasi Material + Lab Tahun Ajaran 2015/2016 -02


Satuan Acara Pengajaran
Mata Kuliah ENMT800005 - Karakterisasi Material + Lab
Pengajar Ir. Sutopo M.Sc.,Ph.D
Nofrijon Bin Imam Sofyan Ph.D
Tujuan Perkuliahan

Minggu Ke 1
Materi Class introduction - About the class - Rules - Grading - Brainstorming
Media LCD Projector
Referensi 1. C.R. Brundle, C.A. Evans, Jr., S. Wilson, Encyclopedia of Materials Characterization, Butterworth-Heinemann, Boston, 1992. 2. B.D Cullity, Elements of X-ray Diffraction, Addison-Wesley Publishing Co. Inc., Massachusetts, 1978. 3. ASM Metals Handbook, Vol 09 - Metallography and Microstructures 4. ASM Metals Handbook, Vol 10 - Materials Characterization 5. S. Amelinckx, D. van Dyck, J. van Landuyt, and G. van Tendeloo: Electron Microscopy Principles and Fundamentals, VCH Verlagsgescllschaft mbH, Weinheim (1997) 6. F.A. Settle: Handbook of Instrumental Techniques for Analytical Chemistry, Prentice Hall PTR (1997)
Aktivitas Lecture Problem solving

 

Minggu Ke 2
Materi Basic in Materials Characterization: Crystal Structure - Crystal system - Plane and direction - Atomic position - Exercise
Media LCD Projector
Referensi B.D. Cullity: Elements of X-ray Diffraction, 2nd ed., Addison-Wesley Publishing Company Inc., Reading, Massachusetts, 1978 C. Hammond: The Basics of Crystallography and Diffraction, 3rd ed., Oxford University Press Inc., New York, 2009. R.J.D. Tilley: Crystals and Crystal Structures, John Wiley & Sons Ltd., Chichester, West Sussex, England, 2006 W.D. Callister, Jr.. Fundamentals of Materials Science and Engineering, John Wiley & Sons, Inc., New York, 2001
Aktivitas Lecture Exercise

 

Minggu Ke 3
Materi Basic in Materials Characterization: Crystal Symmetry - Bravais Lattice - Point Group - Space Group - Notation and Symbol - Exercise
Media LCD Projector
Referensi B.D. Cullity: Elements of X-ray Diffraction, 2nd ed., Addison-Wesley Publishing Company Inc., Reading, Massachusetts, 1978 C. Hammond: The Basics of Crystallography and Diffraction, 3rd ed., Oxford University Press Inc., New York, 2009. R.J.D. Tilley: Crystals and Crystal Structures, John Wiley & Sons Ltd., Chichester, West Sussex, England, 2006 W.D. Callister, Jr.. Fundamentals of Materials Science and Engineering, John Wiley & Sons, Inc., New York, 2001
Aktivitas Lecture Lab preparation

 

Minggu Ke 4
Materi Basic in Materials Characterization: Stereographic Projection - Construction - Wulff Net - Zone Equation - Exercise
Media LCD Projector
Referensi B.D. Cullity: Elements of X-ray Diffraction, 2nd ed., Addison-Wesley Publishing Company Inc., Reading, Massachusetts, 1978 C. Hammond: The Basics of Crystallography and Diffraction, 3rd ed., Oxford University Press Inc., New York, 2009. R.J.D. Tilley: Crystals and Crystal Structures, John Wiley & Sons Ltd., Chichester, West Sussex, England, 2006 W.D. Callister, Jr.. Fundamentals of Materials Science and Engineering, John Wiley & Sons, Inc., New York, 2001
Aktivitas Lecture Exercise

 

Minggu Ke 5
Materi Fundamental Concept in Materials Characterization - Fundamental of X-Ray Diffraction - Diffraction by a Crystal - Bragg's Law - Structural Factor - Exercise
Media LCD Projector
Referensi C. Hammond: The Basics of Crystallography and Diffraction, 3rd Ed., Oxford University Press, 2009. B. D. Cullity: Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., 1978. R.J. D. Tilley: Crystals and Crystal Structures, John Wiley & Sons Ltd., 2006
Aktivitas Lecture Exercise

 

Minggu Ke 6
Materi Lab-1 Preparation of Al - Zn systems: No Zn Al 1 85.0 15.0 2 77.7 22.3 3 55.0 45.0 4 20.0 80.0
Media Lab coat Safety Google Lab equipment
Referensi [1] Thaddesius B. Massalski (Ed), et al., Binary Alloy Phase Diagrams, 2nd Ed. Vol. 1 (1990) 239 ? 241. [2] S Müller, L-W Wang and Alex Zunger, Modelling Simul. Mater. Sci. Eng. 10 (2002) 131 ? 145. [3] B. D. Cullity, Elements of X-Ray Diffraction, 2nd Ed., Addison-Wesley Publishing Co., Inc., Massachusetts (1978) 120, 350 ? 368. [4] P. Villars and L. D. Carvert, Pearson?s Handbook of Crystallographic Data for Intermetalic Phase, Metals Park OH: ASM (1985). [5] Theo Hahn (Ed.), International Tables for Crystallography, Vol. A Space-Group Symetry, IUCr, Kluwer Academic Publisher, (1995).
Aktivitas Laboratorium activity: casting

 

Minggu Ke 7
Materi Lab-2 X-Ray Diffraction: As-cast As-quench Quench-anneal
Media Laboratory equipment XRD
Referensi [1] Thaddesius B. Massalski (Ed), et al., Binary Alloy Phase Diagrams, 2nd Ed. Vol. 1 (1990) 239 ? 241. [2] S Müller, L-W Wang and Alex Zunger, Modelling Simul. Mater. Sci. Eng. 10 (2002) 131 ? 145. [3] B. D. Cullity, Elements of X-Ray Diffraction, 2nd Ed., Addison-Wesley Publishing Co., Inc., Massachusetts (1978) 120, 350 ? 368. [4] P. Villars and L. D. Carvert, Pearson?s Handbook of Crystallographic Data for Intermetalic Phase, Metals Park OH: ASM (1985). [5] Theo Hahn (Ed.), International Tables for Crystallography, Vol. A Space-Group Symetry, IUCr, Kluwer Academic Publisher, (1995).
Aktivitas Specimen Diffractogram from Lab-1

 

Minggu Ke 8
Materi Midterm
Media
Referensi
Aktivitas

 

Minggu Ke 9
Materi Metallography Specimen preparation Sectioning Mounting Grinding Polishing Etching
Media LCD Projector
Referensi 1. Kay Geels: Metallographic and Materialographic Specimen Preparation, Light Microscopy, Image Analysis and Hardness Testing, ASTM International, (2007) 2. Günter Petzow: Metallographic etching: techniques for metallography, ceramography, plastography, ASM International, Materials Park, OH, (1999)
Aktivitas Lecture

 

Minggu Ke 10
Materi Lab-3 SEM/EDX
Media Lab equipment Prepared Specimen
Referensi 1. S. Amelinckx, et al.: Electron Microscopy, Principles and Fundamentals, VCH Verlagsgescllschaft mbH, Weinheim, 1997. 2. C Richard Brundle, Charles A. Evans, Jr., and Shaun Wihon: Encyclopedia of Materials Characterization, Butterworth-Heinemann, MA, 1992. 3. S. J. B. Reed: Electron Microprobe Analysis and scanning electron Microscopy in Geology, Cambridge University Press, Cambridge, 2005.
Aktivitas Microstructure and composition characterization

 

Minggu Ke 11
Materi Project Assignment: Microstructure and Lattice Parameters Change in Al - Zn Alloys
Media Computer/Laptop
Referensi [1] Thaddesius B. Massalski (Ed), et al., Binary Alloy Phase Diagrams, 2nd Ed. Vol. 1 (1990) 239 - 241. [2] S Müller, L-W Wang and Alex Zunger, Modelling Simul. Mater. Sci. Eng. 10 (2002) 131 - 145. [3] B. D. Cullity, Elements of X-Ray Diffraction, 2nd Ed., Addison-Wesley Publishing Co., Inc., Massachusetts (1978) 120, 350 ? 368. [4] P. Villars and L. D. Carvert, Pearson?s Handbook of Crystallographic Data for Intermetalic Phase, Metals Park OH: ASM (1985). [5] Theo Hahn (Ed.), International Tables for Crystallography, Vol. A Space-Group Symetry, IUCr, Kluwer Academic Publisher, (1995).
Aktivitas Journal Writing and Preparation

 

Minggu Ke 12
Materi Thermal Analysis - Introduction - Techniques in Thermal Analysis: TGA, DTA, DSC - Basic Principle - Applications
Media LCD Projector Labcoat in Lab
Referensi 1. Thermal Analysis, Koninklijke Philips Electronics N.V., 2008 2. D.A. Skoog, F.J. Holler and S.R. Crouch: Principles of Instrumental Analysis, Thomson Brooks/Cole, Belmomnt, CA, 2007
Aktivitas Lecture Lab Demo

 

Minggu Ke 13
Materi Particle Size Analyzer - Basic theory - Particle properties - Methods: Sieving Sedimentation Electrozone sensing Microscopy Laser diffraction
Media LCD Projector
Referensi 1. R. Lambourne and T.A. Strivens: Paint and Surface coatings ? Theory and Practice; Woodhead Publishing Ltd., Cambridge, 1999 2. M. Rhodes: Introduction to Particle Technology, 2nd Ed., John Wiley & Sons Ltd., West Sussex, 2008 3. R.B. Gupta and U.B. Kompella: Nanoparticle Technology for Drug Delivery, Taylor & Francis Group, LLC., New York, 2006
Aktivitas Lecture Lab Demo/SEM

 

Minggu Ke 14
Materi Transmission Electron Microscope - Introduction - Basic Theory - Basic Metallography - Sample Preparation - Basic Mechanism in Selected Area Diffraction
Media LCD Projector
Referensi 1. C. Hammond: The Basics of Crystallography and Diffraction, 3rd Ed., Oxford University Press, 2009. 2. B. D. Cullity: Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., 1978. 3. R.J. D. Tilley: Crystals and Crystal Structures, John Wiley & Sons Ltd., 2006
Aktivitas Lecture

 

Minggu Ke 15
Materi Question and Answering Session - Brief topic in one semester - Exercise and solution model
Media LCD Projector
Referensi
Aktivitas Discussion

 

Minggu Ke 16
Materi Final Examination
Media
Referensi
Aktivitas